HRID893596

反应详情

EQUATION

反应方程式

HRID 893596 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 18.85 g of 3-tetradecylphenol, 20 ml of acetic anhydride and 60 ml of pyridine was stirred for 16 hours, then diluted with chloroform, washed with aqueous sodium bicarbonate, dried and the solvent removed by evaporation with toluene, giving 21 g of the desired compound.

WORKUP

后处理

  1. washwashed with aqueous sodium bicarbonate
  2. customdried
  3. customthe solvent removed by evaporation with toluene