1-Phenethylpiperazine → HCID 131716672, compound

HRID 893648Notes

Reaction equation

[C:1]1([CH2:7][CH2:8][N:9]2[CH2:14][CH2:13][NH:12][CH2:11][CH2:10]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:15][CH2:16][C:17]([N:19]1[CH2:24][CH:23]=[C:22]([C:25]2[CH:30]=[CH:29][CH:28]=[C:27]([C:31]([F:34])([F:33])[F:32])[CH:26]=2)[N:21]2[N:35]=[CH:36][C:37]([C:38]#[N:39])=[C:20]12)=[O:18]>>[ClH:15].[ClH:15].[C:1]1([CH2:7][CH2:8][N:9]2[CH2:10][CH2:11][N:12]([CH2:16][C:17]([N:19]3[CH2:24][CH:23]=[C:22]([C:25]4[CH:30]=[CH:29][CH:28]=[C:27]([C:31]([F:34])([F:32])[F:33])[CH:26]=4)[N:21]4[N:35]=[CH:36][C:37]([C:38]#[N:39])=[C:20]34)=[O:18])[CH2:13][CH2:14]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

Reactant 2

HCID 792141-Phenethylpiperazine

HCID 15100972HCID 15100972, compound

Product 1

HCID 131716672HCID 131716672, compound

Procedure

The above compound was prepared by the reaction of 4-(2-phenylethyl)piperazine with the compound of Example 1 by the methods of Examples 16 then 77, mp 235°-237° C.

Sources & evidence

ORD record: ord-463cf84ff0fc4bbd9d190c6303df93e7
Source dataset: uspto-grants-1992_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05126340

Reaction notes

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