HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzonitrile, 4-(trifluoromethyl)- → 4-Methylbenzotrifluoride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzonitrile, 4-(trifluoromethyl)- | HCID 67995 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Methylbenzotrifluoride | HCID 80230 | 91% |
Reaction Steps
To 4 ml of methanol (3.06 g) was added 0.71 g of p-trifluoromethylbenzonitrile. The solution was added to the reactor at 0.34 ml/min. The product, p-trifluoromethyltoluene, was isolated in a methanol solution in a 91% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05126497 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-84acf6a8785148ce8de82354af2abfe6 |
| Source note | uspto-grants-1992_06 |