Potassium Hydroxide → HCID 178464374, compound

HRID 893883Notes

Reaction equation

HRID 893883 reaction equation
F[S:2]([CH2:5][CH2:6][N:7]([CH2:14][CH3:15])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)(=[O:4])=[O:3].[OH-:16].[K+:17]>O>[K:17][CH:5]([S:2]([OH:16])(=[O:4])=[O:3])[CH2:6][N:7]([CH2:14][CH3:15])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 211616872-[Ethyl(phenyl)amino]ethane-1-sulfonyl fluoride

Product 1

HCID 178464374HCID 178464374, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

N-(2-Fluorosulfonylethyl)-N-ethylaniline (22.8 g, 0.1 n) is stirred in water (200 ml) and potassium hydroxide (10 g) for 1-3 hrs. or until thin-layer chromatography shows reaction to be complete. The product is not isolated but is used as an aqueous solution in the coupling reaction.

Workup

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  2. customThe product is not isolated
  3. customis used as an aqueous solution in the coupling reaction

Sources & evidence

ORD record
ord-8d28f0e292b947f9974015a4b4b8c8ca
Source dataset
uspto-grants-1981_08
Patent number
US04282144

Reaction notes

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