Benzoylhydrazine → HCID 178513057, compound

Participants

Reaction Steps

A mixture of 9.1 g (0.07 mole) benzoylhydrazine and 20 ml (28.5 g, 0.16 mole) methyl 2,2,2-trichloroacetimidate was stirred 16 hours at room temperature. The solid that was left was washed with petroleum ether and dried to give 18.6 g (100% yield) of product (mp 170°-172° C.). A sample recrystallized from ethanol had mp 178°-181° C. The structure was confirmed via infrared and elemental analysis.

Provenance & Evidence