HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl N-cyanodithioiminocarbonate → HCID 86736309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl N-cyanodithioiminocarbonate | HCID 66289 | — |
| Reactant | 2-{[(3-Methoxypyridin-2-yl)methyl]sulfanyl}ethan-1-amine | HCID 12951535 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86736309 | HCID 86736309 | 149.6% |
Reaction Steps
A solution of 2-(3-methoxy-2-pyridylmethylthio)-ethylamine (2.1 g) in ethanol (15 ml) was added over one hour to a stirred solution of dimethyl-N-cyanodithioimidocarbonate (1.5 g) in ethanol (15 ml) and the mixture was allowed to stand overnight, to yield on recrystallisation from ethanol/ether N-cyano-N'-[2-(3-methoxy-2-pyridylmethylthio)ethyl]-S-methylisothiourea (2.2 g), m.p. 120°-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04282224 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-0f04be1d88a44abb97612c8f61147953 |
| Source note | uspto-grants-1981_08 |