Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | HCID 21162322 | HCID 21162322 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20528534 | HCID 20528534 | 83% |
Reaction Steps
52.6 parts by weight of 6,10-dimethylundec-2-yl bromide and 27.2 parts by weight of imidazole are dissolved in 80 parts by weight of tetrahydrofuran and the solution is placed in a 250 ml autoclave and heated for 15 hours at 160° C. The reaction product is then filtered and the solvent is removed from the filtrate at atmospheric pressure. Distillation in vacuo of the residue obtained gives 41.5 parts by weight (83% of theory) of 1-(1,5,9-trimethyldecyl)-imidazole; b.p.: 185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04282238 |
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| Source dataset | uspto-grants-1981_08 |
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| ORD ID | ord-10cfce75e9b443dfae86c3adf71ae093 |
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| Source note | uspto-grants-1981_08 |
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