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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 893974Generated: October 30, 2026

Imidazole → HCID 20528534, compound

https://huagongshe.com/reaction/893974

Reaction equation

Participants

RoleNameHCIDCharge
ReactantImidazoleHCID 795—
ReactantHCID 21162322HCID 21162322—
SolventTetrahydrofuranHCID 8028—
ProductHCID 20528534HCID 2052853483%

Reaction Conditions

Temperature160 °C

Reaction Steps

52.6 parts by weight of 6,10-dimethylundec-2-yl bromide and 27.2 parts by weight of imidazole are dissolved in 80 parts by weight of tetrahydrofuran and the solution is placed in a 250 ml autoclave and heated for 15 hours at 160° C. The reaction product is then filtered and the solvent is removed from the filtrate at atmospheric pressure. Distillation in vacuo of the residue obtained gives 41.5 parts by weight (83% of theory) of 1-(1,5,9-trimethyldecyl)-imidazole; b.p.: 185° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04282238
Source datasetuspto-grants-1981_08
ORD IDord-10cfce75e9b443dfae86c3adf71ae093
Source noteuspto-grants-1981_08