Phosphorus sulfide (P2S5) → HCID 178433677, compound

HRID 893986Notes

Reaction equation

HRID 893986 reaction equation
[CH3:1][C:2]1[NH:6][CH:5]=[N:4][C:3]=1[CH2:7][S:8][CH2:9][CH2:10][NH:11][C:12](=[NH:20])[C:13]1[CH:18]=[CH:17][C:16](O)=[CH:15][CH:14]=1.P12(SP3(SP(SP(S3)(S1)=S)(=S)S2)=S)=[S:22]>N1C=CC=CC=1>[CH3:1][C:2]1[NH:6][CH:5]=[N:4][C:3]=1[CH2:7][S:8][CH2:9][CH2:10][NH:11][C:12](=[NH:20])[C:13]1[CH:18]=[CH:17][C:16]([SH:22])=[CH:15][CH:14]=1

Participants

4

Reactant 2

HCID 14817Phosphorus sulfide (P2S5)HCID 178433676HCID 178433676, compound

Product 1

HCID 178433677HCID 178433677, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

N-[2-(5-Methyl-4-imidazolylmethylthio)ethyl]-4-hydroxybenzamidine and a slight excess of phosphorus pentasulphide were refluxed in pyridine for 45 minutes to give the title compound.

Sources & evidence

ORD record
ord-bc38ff95a6b84df2b31b5f8069e22cdb
Source dataset
uspto-grants-1981_08
Patent number
US04282234

Reaction notes

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