HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → 2,5-Dichlorobenzenesulfenyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 2,5-Dichlorobenzenethiol | HCID 79965 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 2,5-Dichlorobenzenesulfenyl chloride | HCID 12878541 | 85.6% |
Reaction Steps
The procedure of Example 13 was repeated, reacting a slurry of N-chlorosuccinimide (3.72 g., 27.9 mmoles) in 50 ml. of carbon tetrachloride with 2,5-dichlorothiophenol (5.0 g., 27.9 mmoles) in 25 ml. of carbon tetrachloride. 2,5-Dichlorobenzenesulfenyl chloride (5.1 g.) was isolated as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04282242 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-a9001844d3b24ac096a12e8a7ce68f90 |
| Source note | uspto-grants-1981_08 |