Sodium Methoxide → HCID 23709004, compound

HRID 894083Notes

Reaction equation

HRID 894083 reaction equation
[CH3:1][N:2]1[C:6]([C:7](=[O:14])[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:5][C:4]([C:15]([O-:17])=[O:16])=[CH:3]1.C[O-].[Na+:20]>CC(C)=O>[CH3:1][N:2]1[C:6]([C:7](=[O:14])[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:5][C:4]([C:15]([O-:17])=[O:16])=[CH:3]1.[Na+:20]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 20401017HCID 20401017, compound

Product 1

HCID 23709004HCID 23709004, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

1-Methyl-5-benzoylpyrrole-3-carboxylate is dissolved by warming in acetone. An equivalent of sodium methoxide is added with stirring. Sodium 1-methyl-5-benzoylpyrrole-3-carboxylate is isolated by evaporation to dryness or by precipitation resulting from addition of a non-solvent (ether or pentane).

Sources & evidence

ORD record
ord-be5c12620e71417dabd8f299d9471b4a
Source dataset
uspto-grants-1981_08
Patent number
US04282242

Reaction notes

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