Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3',5'-Dichloro-2'-hydroxyacetophenone → 2,4-Dichloro-6-(1'-hydroxyethyl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3',5'-Dichloro-2'-hydroxyacetophenone | HCID 520608 | — |
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2,4-Dichloro-6-(1'-hydroxyethyl)phenol | HCID 21162831 | 79.2% |
반응 단계
3,5-Dichloro-2-hydroxyacetophenone (40 g) was treated in ethanol with sodium borohydride (4 g). The solid reaction product was recrystallized from benzene to give 2,4-dichloro-6-(1'-hydroxy ethyl) phenol (32 g, m.p. 70°).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04282390 |
| 출처 데이터셋 | uspto-grants-1981_08 |
| ORD ID | ord-09bbc22672b540f3bb76d10ec4c56923 |
| 출처 메모 | uspto-grants-1981_08 |