HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorothiophenol → HCID 21162467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorothiophenol | HCID 16257 | — |
| Reactant | 5-Bromofuran-3-carboxylic acid | HCID 13333560 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21162467 | HCID 21162467 | — |
Reaction Steps
Following the procedure of Example 11, except for use of two 50 ml. quantities of dimethylformamide, 3-chlorothiophenol (4.52 g., 31.4 mmoles) was reacted with 5-bromofuran-3-carboxylic acid to yield crude product (1.9 g.). Recrystallization from hot hexane gave purified 5-(3-chlorophenylthio)furan-3-carboxylic acid (1.0 g., m.p. 98°-102° C., m/e 254).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04282246 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-2bcb0ec34dca407c9aa256b8a6594717 |
| Source note | uspto-grants-1981_08 |