Sodium Methoxide → HCID 23720705, compound

HRID 894256Notes

Reaction equation

HRID 894256 reaction equation
[C:1]1([S:7][CH2:8][C:9]2[O:13][C:12]([C:14]([O-:16])=[O:15])=[CH:11][CH:10]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C[O-].[Na+:19]>CC(C)=O>[C:1]1([S:7][CH2:8][C:9]2[O:13][C:12]([C:14]([O-:16])=[O:15])=[CH:11][CH:10]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1.[Na+:19]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 21162526HCID 21162526, compound

Product 1

HCID 23720705HCID 23720705, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

5-Phenylthiomethylfuran-2-carboxylate is dissolved by warming in acetone. An equivalent of sodium methoxide is added with stirring. Sodium 5-phenylthiomethylfuran-2-carboxylate is isolated by evaporation to dryness or by precipitation resulting from addition of a non-solvent (ether or pentane).

Sources & evidence

ORD record
ord-e2156165c176475481636740f9ffbfb0
Source dataset
uspto-grants-1981_08
Patent number
US04282246

Reaction notes

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