Heptane → HCID 178506989, compound

HRID 894257Notes

Reaction equation

HRID 894257 reaction equation
[C:1]1([C:7]2[S:11][C:10]([C:12]([O-:14])=[S:13])=[CH:9][CH:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C([O-])(=O)CCCCCCC/C=C\CCCCCCCC.[Mg+2:35].C([O-])(=O)CCCCCCC/C=C\CCCCCCCC.CCCCCCC>C(O)C>[C:1]1([C:7]2[S:11][C:10]([C:12]([O-:14])=[S:13])=[CH:9][CH:8]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1.[Mg+2:35].[C:1]1([C:7]2[S:11][C:10]([C:12]([O-:14])=[S:13])=[CH:9][CH:8]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

5

Reactant 3

HCID 8900HeptaneHCID 64332821555-53-9HCID 178526128HCID 178526128, compound

Product 1

HCID 178506989HCID 178506989, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

5-Phenylthiothiophene-2-carboxylate and an equivalent quantity of magnesium oleate are each dissolved in ethanol and the solutions mixed. Magnesium 5-phenylthiothiophene-2-carboxylate is isolated by concentration and/or addition of heptane.

Workup

  1. additionthe solutions mixed

Sources & evidence

ORD record
ord-640e1d2c4c704203869b5e1f9e7c8f54
Source dataset
uspto-grants-1981_08
Patent number
US04282246

Reaction notes

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