HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzenethiol → p-Toluenesulfenyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzenethiol | HCID 7811 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | p-Toluenesulfenyl chloride | HCID 11019146 | 88.2% |
Reaction Steps
By the method of Preparation 5, 6.2 g. of p-toluenethiol (6.2 g., 50 mmoles) was reacted with N-chlorosuccinimide (6.67 g., 50 mmoles) in 100 ml. of benzene to yield p-toluenesulfenyl chloride (7.0 g.) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04282246 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-74d7decd008644929a1e533342bb9a0a |
| Source note | uspto-grants-1981_08 |