Allyl Isothiocyanate → HCID 12889653, compound

HRID 894323Notes

Reaction equation

HRID 894323 reaction equation
[F:1][C:2]1[CH:10]=[CH:9][C:5]([CH:6]=[N:7][OH:8])=[CH:4][CH:3]=1.[CH2:11]([N:14]=[C:15]=[S:16])[CH:12]=[CH2:13]>>[F:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]2[CH2:13][CH:12]([CH2:11][N:14]=[C:15]=[S:16])[O:8][N:7]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 5971Allyl IsothiocyanateHCID 68017N-[(4-fluorophenyl)methylidene]hydroxylamine

Product 1

HCID 12889653HCID 12889653, compound

Procedure

A 12.5 g. portion of 4-fluorobenzaldoxime was chlorinated and reacted with 50 ml. of allylisothiocyanate to prepare 3.4 g. of product, m.p. 59°-61°.

Workup

  1. customreacted with 50 ml

Sources & evidence

ORD record
ord-2fa846c20d60445da3c01d759c823df1
Source dataset
uspto-grants-1981_08
Patent number
US04283403

Reaction notes

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