HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Fluoro-3-phenoxybenzylbromide → alpha-Fluoro-3-phenoxybenzyl alpha-isopropyl-(3,4-dichlorophenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Fluoro-3-phenoxybenzylbromide | HCID 13194583 | — |
| Reactant | 2-(3,4-Dichlorophenyl)-3-methylbutanoic acid | HCID 20507330 | — |
| Product | alpha-Fluoro-3-phenoxybenzyl alpha-isopropyl-(3,4-dichlorophenyl)acetate | HCID 53806714 | — |
Reaction Steps
This compound was prepared from α-isopropyl-(3,4-dichlorophenyl)acetic acid and α-fluoro-3-phenoxybenzyl bromide following the procedure described in Example 2 Method B. The product, a colourless oil, was characterised by pmr spectroscopy. Chemical shift δ ppm (solvent CDCl3): 0.76(3H, d, J=6Hz, CH3); 1.07(3H, d of d, J=6Hz and J=2Hz, CH3); 2.33(1H, m, --CH(CH3)2); 3.28(1H, d, J=10Hz, CH); 7.24(1H, d of d, J=56Hz and J=2Hz, CHF) and about 7.33(12H, m, aromatic protons).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04283414 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-8dcb370ba4d047609536e90909360921 |
| Source note | uspto-grants-1981_08 |