HCID 20536381, compound → HCID 20536377, compound

HRID 894461Notes

Reaction equation

HRID 894461 reaction equation
[OH:1][CH:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[N:6]2[CH2:13][CH2:14][NH:15][CH2:16][CH:5]2[C:4]2[CH:17]=[CH:18][CH:19]=[CH:20][C:3]1=2.[CH2:21]([OH:23])C.[CH3:24]C(C)=O>>[OH:1][CH:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[N:6]2[CH2:13][CH2:14][N:15]([CH3:24])[CH2:16][CH:5]2[C:4]2[C:17]([O:23][CH3:21])=[CH:18][CH:19]=[CH:20][C:3]1=2

Participants

3

Reactant 2

HCID 20536381HCID 20536381, compoundHCID 21889777Acetone ethanol

Product 1

HCID 20536377HCID 20536377, compound

Procedure

10-hydroxy-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepine, (cis configuration), Rf in ethanol:acetone (9:1)=0.43 on SiO2, m.p. 217° C.

Sources & evidence

ORD record
ord-74c3d13206b44574a773af60e01e7d76
Source dataset
uspto-grants-1981_08
Patent number
US04284559

Reaction notes

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