Water → HCID 12926287, compound

Participants

Reaction Steps

10 g of N-(1'-phenoxy-2',2',2'-trichloroethyl)-2-hydroxybenzamide and 5.2 g of phenyl chlorocarbonate were dissolved in 200 ml of acetone and the solution was kept at a temperature below 10° C. with an ice-water bath. 3.3 g of triethylamine were added dropwise thereto under stirring and the reaction was continued at room temperature for a further period of three hours. The reaction mixture was poured into water and the resulting crystals were recrystallized from methanol to obtain 5.2 g of N-(1'-phenoxy-2',2',2'-trichloroethyl)-2-phenoxycarbonyloxybenzamide as which crystals.

Provenance & Evidence