Perchloric Acid → HCID 85884985, compound

Participants

Reaction Steps

To 1-n-butylimidazole (0.31 g; 0.0025 mole) in methanol (5 ml) was added perchloric acid (0.33 g, 70%) in methanol (3 ml). After boiling for 5 minutes, the mixture was evaporated under reduced pressure to afford a white solid. Recrystallisation of the solid from ethyl acetate/ether (1:4) afforded 1-n-butylimidazole perchlorate as a white solid, m.p. 54° to 55° C. (Found: C,37.25; H,5.95; N,12.55. Calc. for C7H13ClN2O4 : C,37.4; H,5.8; N,12.45).

Provenance & Evidence