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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 894548Generated: October 25, 2026

1-Cyano-2-ethoxy-2-methylaminoethylene → HCID 178483853, compound

https://huagongshe.com/reaction/894548

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Cyano-2-ethoxy-2-methylaminoethyleneHCID 73683202—
ReactantHCID 178433288HCID 178433288—
SolventPyridineHCID 1049—
ProductHCID 178483853HCID 178483853—

Reaction Steps

4-Methyl-5-[(2-aminoethyl)thiomethyl]imidazole (3.5 g) was added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene in pyridine (3.1 g) and the solution was stirred for 5 hours at 100°. The product was chromatographed on a column of neutral alumina with elution by chloroform/ethyl acetate (1:1) to give the title compound as a glass.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04284640
Source datasetuspto-grants-1981_08
ORD IDord-50434325540842ad8efa31b7e0e23544
Source noteuspto-grants-1981_08