Ethylamine → 1-Nitro-2-ethylamino-2-[2-(3-isothiazolylmethylthio)ethylamino]ethylene

HRID 894572Notes

Reaction equation

[N+:1]([CH:4]=[C:5](SC)[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[CH:15]=[CH:14][S:13][N:12]=1)([O-:3])=[O:2].[CH2:18]([NH2:20])[CH3:19]>>[N+:1]([CH:4]=[C:5]([NH:20][CH2:18][CH3:19])[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[CH:15]=[CH:14][S:13][N:12]=1)([O-:3])=[O:2]

Participants

Reactant 2

HCID 6341Ethylamine

HCID 705418951-Nitro-2-methylthio-2-[2-(3-isothiazolylmethylthio)ethylamino]ethylene

Product 1

HCID 705445711-Nitro-2-ethylamino-2-[2-(3-isothiazolylmethylthio)ethylamino]ethylene

Procedure

Reaction of 1-nitro-2-methylthio-2-[2-(3-isothiazolylmethylthio)ethylamino]ethylene (see Example 72(ii)) with ethylamine by the procedure of Example 8(ii) gives the title product.

Sources & evidence

ORD record: ord-6ba1984bb2ef41b98547dc907f2a78c6
Source dataset: uspto-grants-1981_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04284640

Reaction notes

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