HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Bis(methylthio)-2-nitroethylene → 1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | HCID 178510963 | HCID 178510963 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene | HCID 178503821 | — |
Reaction Steps
Reaction of 5-bromo-4-(4-aminobutyl)imidazole with 1-nitro-2,2-bis-methylthioethylene in the procedure of Example 8(i) yields 1-nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene, m.p. 157°-158°, (from isopropanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04284640 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-2b1e70ec06d541aa9cbb54bc743ecbe9 |
| Source note | uspto-grants-1981_08 |