2,3-Dimethylaniline → HCID 20512419, compound

HRID 894588Notes

Reaction equation

HRID 894588 reaction equation
Br[CH:2]([CH3:13])[CH2:3][NH:4][C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([CH3:11])[C:6]=1[CH3:12].[CH3:14][C:15]1[C:21]([CH3:22])=[CH:20][CH:19]=[CH:18][C:16]=1[NH2:17]>>[CH3:12][C:6]1[C:7]([CH3:11])=[CH:8][CH:9]=[CH:10][C:5]=1[NH:4][CH2:3][CH:2]([NH:17][C:16]1[CH:18]=[CH:19][CH:20]=[C:21]([CH3:22])[C:15]=1[CH3:14])[CH3:13]

Participants

3

Reactant 2

HCID 68932,3-DimethylanilineHCID 20512465HCID 20512465, compound

Product 1

HCID 20512419HCID 20512419, compoundYield 84.2%

Procedure

N-(β-Bromopropyl)-2,3-dimethyl-aniline, prepared as indicated in point (b) above, is reacted with 2,3-dimethylaniline as given in Example 3, Method (c), point (b) to obtain 1,2-bis(2',3'-dimethylphenyl-amino)-propane with a yield of 84.2%. The hydrobromide of the product melts at 204°-208° C.

Sources & evidence

ORD record
ord-f59ea43558ce42fb8feb4b958d398d3b
Source dataset
uspto-grants-1981_08
Patent number
US04284642

Reaction notes

Loading…