Aniline → HCID 20512448, compound

HRID 894606Notes

Reaction equation

HRID 894606 reaction equation
CC1C=CC=C(C)C=1[CH:9]([NH2:18])C(C1C=CC=CC=1)C.Br[CH:20]([CH3:31])[CH2:21][NH:22][C:23]1[C:28]([CH3:29])=[CH:27][CH:26]=[CH:25][C:24]=1[CH3:30].[NH2:32][C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1>>[CH3:30][C:24]1[CH:25]=[CH:26][CH:27]=[C:28]([CH3:29])[C:23]=1[N:22]1[CH2:21][CH:20]([CH3:31])[N:32]([C:33]2[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=2)[C:9]1=[NH:18]

Participants

4

Reactant 3

HCID 6115AnilineHCID 20512395HCID 20512395, compoundHCID 86737945HCID 86737945, compound

Product 1

HCID 20512448HCID 20512448, compound

Procedure

1-(2',6'-Dimethylphenyl)-2-phenyl-amino-propane, applied as starting substance, is prepared with a yield of 41.0% by reacting N-(β-bromopropyl)-2,6-dimethyl-aniline, a compound obtained as described in Example 3, Method (c), point (a), with aniline according to the process given in Example 3, Method (c), point (b). The boiling point of the product is 116°-120° C./1.5 mm Hg.

Workup

  1. customis prepared with a yield of 41.0%
  2. customa compound obtained
  3. customis 116°-120° C.

Sources & evidence

ORD record
ord-f59ffe48e50e4ac980a694a02679650f
Source dataset
uspto-grants-1981_08
Patent number
US04284642

Reaction notes

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