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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 894681Generated: November 2, 2026

Acetic Acid → HCID 20277286, compound

https://huagongshe.com/reaction/894681

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium AcetateHCID 517045—
ReactantHCID 20277346HCID 20277346—
SolventAcetic AnhydrideHCID 7918—
ProductHCID 20277286HCID 20277286—

Reaction Steps

Starting from a mixture of diethyl 2-methyl-4-(2-nitrophenyl)-6-formylmethyl-1,4-dihydropyridine-3,5-dicarboxylate, hydroxylamine hydrochloride and sodium acetate in acetic acid and acetic anhydride, was obtained an oil of diethyl 2-methyl-4-(2-nitrophenyl)-6-cyanomethyl-1,4-dihydropyridine-3,5-dicarboxylate, by applying an essentially similar manner to that of Example 4-(2).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04284634
Source datasetuspto-grants-1981_08
ORD IDord-514dea12ce6e4fd389adf553e4b13287
Source noteuspto-grants-1981_08