HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 54051668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromoethyl ethyl ether | HCID 61141 | — |
| Reactant | HCID 178472877 | HCID 178472877 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54051668 | HCID 54051668 | 97.7% |
Reaction Steps
Ethyl 2-hydroxyimino-3-oxobutyrate (syn isomer 40 g.), ethoxyethyl bromide (41.1 g.), potassium carbonate (54.1 g.), N,N-dimethylformamide (65 ml.) and ethylacetate (65 ml.) were treated in a similar manner to that of Example A-(1) to give ethyl 2-(2-ethoxyethoxyimino)-3-oxobutyrate (syn isomer, 56.8 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04284631 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-5100a9668fe042c789bec13099863e55 |
| Source note | uspto-grants-1981_08 |