HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 894767Generated: October 30, 2026
HCID 23315738, compound → HCID 23315735, compound
https://huagongshe.com/reaction/894767
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 23315738 | HCID 23315738 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23315735 | HCID 23315735 | 83.1% |
Reaction Steps
A mixture of N-(4-chloromethylbenzyloxy)-phthalimide (18.5 g.) and potassium phthalimide (15.4 g.) in N,N-dimethylformamide (180 ml.) was stirred at 60° C. for 5 hours. The mixture was poured into ice-water and the precipitates were collected by filtration. The precipitates were washed with water and acetone in turn to give N-(4-phthalimidomethylbenzyloxy)-phthalimide (21.0 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04284631 |
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| Source dataset | uspto-grants-1981_08 |
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| ORD ID | ord-cd76ebc8b1b34d7fbfc9d270dc93d931 |
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| Source note | uspto-grants-1981_08 |
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