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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 894767Generated: October 30, 2026

HCID 23315738, compound → HCID 23315735, compound

https://huagongshe.com/reaction/894767

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23315738HCID 23315738—
ReactantPhthalimide potassium saltHCID 24194345—
SolventDimethylformamideHCID 6228—
ProductHCID 23315735HCID 2331573583.1%

Reaction Conditions

Temperature60 °C

Reaction Steps

A mixture of N-(4-chloromethylbenzyloxy)-phthalimide (18.5 g.) and potassium phthalimide (15.4 g.) in N,N-dimethylformamide (180 ml.) was stirred at 60° C. for 5 hours. The mixture was poured into ice-water and the precipitates were collected by filtration. The precipitates were washed with water and acetone in turn to give N-(4-phthalimidomethylbenzyloxy)-phthalimide (21.0 g.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04284631
Source datasetuspto-grants-1981_08
ORD IDord-cd76ebc8b1b34d7fbfc9d270dc93d931
Source noteuspto-grants-1981_08