HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 2763630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 2,4-Dichlorobenzyl chloride | HCID 7212 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178472877 | HCID 178472877 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 2763630 | HCID 2763630 | 99.2% |
Reaction Steps
Ethyl 2-hydroxyimino-3-oxobutyrate (syn isomer, 17.0 g.), 2,4-dichlorobenzyl chloride (25 g.), potassium carbonate (22.0 g.), N,N-dimethylformamide (25 ml.) and ethyl acetate (25 ml.) were treated in a similar manner to that of Example A - (1) to give ethyl 2-(2,4-dichlorobenzyloxyimino)-3-oxobutyrate (syn isomer, 33.7 g.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04284631 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-59da5a84657a42d38b96cd09c54065b8 |
| Source note | uspto-grants-1981_08 |