HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octene → Gamma-Decalactone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octene | HCID 8125 | — |
| Reactant | Potassium Acetate | HCID 517044 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Gamma-Decalactone | HCID 12813 | 48% |
Reaction Steps
Octene-1 in an amount of 2.2 g. and 23.6 g. of ceric ammonium nitrate, Ce(NH4)2 (NO3)6, were refluxed under nitrogen in 200 ml. glacial acetic acid containing 60 g. potassium acetate for less than 0.5 hour, there being obtained a 48% yield of gamma-n-hexyl-butyrolactone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04285868 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-d3b422afcd654766adc972a2936b49dd |
| Source note | uspto-grants-1981_08 |