HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenoxybenzyl alcohol → 3-Phenoxybenzyl 2-(4-chlorophenylamino)-3-methylbutanimidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenoxybenzyl alcohol | HCID 26295 | — |
| Reactant | Methyl 2-(4-chlorophenylamino)-3-methylbutanimidate | HCID 12767220 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Phenoxybenzyl 2-(4-chlorophenylamino)-3-methylbutanimidate | HCID 12767221 | — |
Reaction Steps
A solution of 2.25 g (10 mmol) of methyl 2-(4- chlorophenylamino)-3-methylbutanimidate and 4.00 g (20 mmol) of 3-phenoxybenzyl alcohol is heated with continuous removal of methanol. Upon cessation of methanol evolution, there is obtained an oil, 3-phenoxybenzyl 2-(4-chlorophenylamino)-3-methylbutanimidate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04285879 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-ba3776f3e8244b6da37210239895a46e |
| Source note | uspto-grants-1981_08 |