HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-N,N-dimethylethylamine → 1-(Dimethylamino-ethoxyimino)cyclododecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-N,N-dimethylethylamine | HCID 7901 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Cyclododecanone, oxime | HCID 136762 | — |
| Reactant | Fumarate(1-) | HCID 6183479 | — |
| Product | 1-(Dimethylamino-ethoxyimino)cyclododecane | HCID 13205802 | — |
Reaction Steps
Starting from 2.4 g. (0.1 moles) of sodium hydride, 19.73 g. (0.1 moles) of cyclododecanone oxime and 11.8 g. (0.11 moles) of 1-dimethylamino-2-chloroethane the title compound is prepared as in Example 1. Yield: 19.5 g. (72.65%). Hydrogen fumarate, m.p.: 108°-110° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04285942 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-2a927a9e8b7c4c3ebc0cce06e6c0ad45 |
| Source note | uspto-grants-1981_08 |