HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 1-(Diisopropylamino-propoxyimino)cyclododecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Cyclododecanone, oxime | HCID 136762 | — |
| Reactant | Fumarate(1-) | HCID 6183479 | — |
| Reactant | 1-Diisopropylamino-3-chloropropane | HCID 12935431 | — |
| Product | 1-(Diisopropylamino-propoxyimino)cyclododecane | HCID 13205812 | — |
Reaction Steps
Starting from 19.7 g. (0.1 moles) of cyclododecanone oxime, 2.4 g. (0.1 moles) of sodium hydride and 19.55 g. (0.11 moles) of 1-diisopropylamino-3-chloropropane the title product is prepared as in Example 1. Yield: 24.2 g. (71.6%). Hydrogen fumarate, m.p.: 119°-121° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04285942 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-7dea3b45d4f84f28bd7f35aa84ae0d0f |
| Source note | uspto-grants-1981_08 |