HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclododecanone → 1-(Dimethylamino-propoxyimino)cyclododecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclododecanone | HCID 13246 | — |
| Reactant | Fumarate(1-) | HCID 6183479 | — |
| Reactant | O-(3-(dimethylamino)propyl)hydroxylamine dihydrochloride | HCID 21884286 | — |
| Product | 1-(Dimethylamino-propoxyimino)cyclododecane | HCID 13205801 | — |
Reaction Steps
Starting from 18.23 g. (0.1 moles) of cyclododecanone and 21.0 g. (0.11 moles) of dimethylaminopropoxyamine dihydrochloride the title compound is prepared as in Example 13. Yield: 20.9 g. (74%). Hydrogen fumarate, m.p.: 117°-118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04285942 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-ffc81a4867ab4582a30f57af21e9fe3a |
| Source note | uspto-grants-1981_08 |