HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 178525423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 11-{[(Methylsulfanyl)carbonothioyl]amino}undecanoic acid | HCID 20574078 | — |
| Product | HCID 178525423 | HCID 178525423 | — |
Reaction Steps
Methyl 10-carboxydecyldithiocarbamate (28 g., 0.096 mol.) was reacted with 6.5 g. (0.1 mol.) of sodium azide according to the procedure described in Example 7. Acidification upon work-up gave 1-(10-carboxydecyl)tetrazole-5-thiol as a white precipitate, m.p. 95°-98°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04286089 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-de6302bb3ee4464a960dfc0093d05878 |
| Source note | uspto-grants-1981_08 |