HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-methoxy-6-(4-methoxyphenyl)naphthalene → 1-Chloro-6-(4-hydroxyphenyl)-2-naphthol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-methoxy-6-(4-methoxyphenyl)naphthalene | HCID 11162335 | — |
| Reactant | Pyridinium hydrochloride | HCID 21584435 | — |
| Product | 1-Chloro-6-(4-hydroxyphenyl)-2-naphthol | HCID 6102690 | — |
Reaction Steps
The title compound was prepared by reacting 1-chloro-2-methoxy-6-(4-methoxyphenyl)naphthalene (0.32 g, 1.07 mmol) with pyridinium HCl (7 g) at 190° C. according to method B to yield 0.12 g (41%) of an off white solid: mp 222-224° C. (dec.);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06914074B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-e71de5fa2a594b95ab954da6a586fd94 |
| Source note | uspto-grants-2005_07 |