2,5-Dimethylpyrrolidine → HCID 22352629, compound

HRID 895301Notes

Reaction equation

HRID 895301 reaction equation
Cl[C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][CH:5]=[C:4]([O:11][CH3:12])[N:3]=1.[CH3:13][CH:14]1[CH2:18][CH2:17][CH:16]([CH3:19])[NH:15]1>C(O)C>[CH3:13][CH:14]1[CH2:18][CH2:17][CH:16]([CH3:19])[N:15]1[C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][CH:5]=[C:4]([O:11][CH3:12])[N:3]=1

Participants

4

Reactant 2

HCID 960342,5-DimethylpyrrolidineHCID 27950292-Chloro-6-methoxy-3-nitropyridine

Product 1

HCID 22352629HCID 22352629, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

4 g (0.0212 mol) of the product 2-chloro-3-nitro-6-methoxypyridine, 40 ml of ethanol and 4.2 g (0.042 mol) of 2,5-dimethylpyrrolidine were placed in a fully equipped round-bottomed flask.

Sources & evidence

ORD record
ord-aa8a63d9040949ef8a68e5db947f9439
Source dataset
uspto-grants-2005_07
Patent number
US06916345B2

Reaction notes

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