Cyclohexene → HCID 12093404, compound

HRID 895305Notes

Reaction equation

HRID 895305 reaction equation
[CH3:1][O:2][C:3]1[N:8]=[C:7]([N:9]2[CH2:14][CH2:13][N:12]([CH3:15])[CH2:11][CH2:10]2)[C:6]([N+:16]([O-])=O)=[CH:5][CH:4]=1.C1CCCCC=1>[Pd].C(O)C>[CH3:1][O:2][C:3]1[N:8]=[C:7]([N:9]2[CH2:14][CH2:13][N:12]([CH3:15])[CH2:11][CH2:10]2)[C:6]([NH2:16])=[CH:5][CH:4]=1

Participants

5

Reactant 2

HCID 8079CyclohexeneHCID 22352628HCID 22352628, compound

Product 1

HCID 12093404HCID 12093404, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

1.30 g (0.0052 mol) of the product 1-(6-methoxy-3-nitropyrid-2-yl)-4-methylpiperazine synthesized according to the above procedure, 25 ml of ethanol, 5 ml of cyclohexene and 0.6 g of palladium-on-charcoal were placed in a fully equipped round-bottomed flask.

Sources & evidence

ORD record
ord-2c9affcd527d420f8e2d64c8f2d0fb93
Source dataset
uspto-grants-2005_07
Patent number
US06916345B2

Reaction notes

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