HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthalenesulfonyl chloride → HCID 9954461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthalenesulfonyl chloride | HCID 66560 | — |
| Reactant | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Reactant | HCID 9837669 | HCID 9837669 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9954461 | HCID 9954461 | — |
Reaction Steps
from 3-(octahydro-7-indolizinyl)-1-H-5-azaindole (more polar isomer) (8 mg, 0.033 mmol), 1-naphthalenesulfonyl chloride (15 mg, 0.072 mmol) and 1M NaN(TMS)2 (100 μL, 0.10 mmol) in THF (0.5 mL) at RT.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06916818B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-3aef10e7f50b4b4e896f7dc135e3856d |
| Source note | uspto-grants-2005_07 |