Benzoyl chloride → HCID 22379856, compound

HRID 895445Notes

Reaction equation

HRID 895445 reaction equation
CN1[CH2:7][CH:6]=[C:5]([C:8]2[C:16]3[C:11](=[N:12][CH:13]=[CH:14][CH:15]=3)[NH:10][CH:9]=2)CC1.[C:17](Cl)(=[O:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:17]([N:10]1[C:11]2[C:16](=[CH:15][CH:14]=[CH:13][N:12]=2)[C:8]([CH:5]2[CH2:6][CH:7]=[CH:8][CH2:9][N:10]2[CH3:11])=[CH:9]1)(=[O:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 7412Benzoyl chlorideHCID 120962783-(1-Methyl-1,2,3,6-tetrahydropyridin-4-yl)-1H-pyrrolo[2,3-b]pyridine

Product 1

HCID 22379856HCID 22379856, compound

Procedure

(6.7 mg, 18%); from 3-(1-methyl-1,2,3,6-tetrahydro-4-pyridinyl)-1H-7-azaindole (25.0 mg, 0.12 mmol) and benzoyl chloride (28 μL, 0.24 mmol); HRMS-FAB+for C20H19N3O: calculated MH+:318.16064; found:318.16191.

Sources & evidence

ORD record
ord-02baa0ce19ac46958c3d21e02f51b567
Source dataset
uspto-grants-2005_07
Patent number
US06916818B2

Reaction notes

Loading…