HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 895502Generated: October 31, 2026
O-Phenylenediamine → HCID 11289659, compound
https://huagongshe.com/reaction/895502
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18951130 | HCID 18951130 | — |
| Product | HCID 11289659 | HCID 11289659 | — |
Reaction Steps
Ortho-phenylenediamine is treated with a suitably substituted bromoacetic acid derivative, such as 2-bromo-2-(3-bromophenyl)acetic acid, in basic medium, such as aqueous sodium hydroxide, which upon warming to 60° C. and then maintaining at this temperature for 30 minutes, affords the product 3-(3-bromophenyl)-1,2,3,4-tetrahydro-2-quinoxalinone as a precipitate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06916805B2 |
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| Source dataset | uspto-grants-2005_07 |
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| ORD ID | ord-c5d93a68e4da4d65a06ae9c5c30219ce |
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| Source note | uspto-grants-2005_07 |
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