3,3-Dimethylbutanoyl chloride → HCID 69742557, compound

Participants

Reaction Steps

By following the above procedure and using neopentylcarbonyl chloride, and (3R,4R)-4-phenyl-3-triethylsilyloxy-azetidin-2-one were converted to the title product: 1H NMR (CDCl3) δ 0.19-0.62 (m, 15H), 0.88 (s, 3H), 2.43 (d, 1H, J=13.8 Hz), 2.62 (d, 1H, J=14.1 Hz), 4.90 (d, 1H, J=5.7 Hz), 4.95 (d, 1H, J=6.0 Hz), 7.05-7.17 (m, 5H).

Provenance & Evidence