HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Dimethylpiperidine → HCID 60017453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Dimethylpiperidine | HCID 70942 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 11772697 | HCID 11772697 | — |
| Product | HCID 60017453 | HCID 60017453 | — |
Reaction Steps
(20S)-3β-hydroxy-4,4,20-trimethyl-pregna-8,14-dien-21-al was treated with 3,3-dimethyl-piperidine and sodium tris(acetoxy)borohydride as described in Example 1h). (20S)-20-[(3,3-dimethylpiperidin-1-yl)methyl]-4,4-dimethyl-5α-pregna-8,14-dien-3β-ol was isolated as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06916921B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-ea808e9914a84268b065d78c2db36dd5 |
| Source note | uspto-grants-2005_07 |