HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malononitrile → HCID 5061445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | 3-(4-Methoxyphenyl)prop-2-enal | HCID 230995 | — |
| Catalyst | Piperidine | HCID 8082 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 5061445 | HCID 5061445 | 90.7% |
Reaction Steps
To 0.52 g (3.2 mmol) of the aldehyde from step (a) and 0.26 g (4 mmol) malononitrile in 30 ml ethanol was added 2 drops piperidine and the reaction mixture was refluxed for 40 minutes, cooled, filtered and washed with ethanol to yield 0.61 g (90% yield) of an orange solid, m.p. 160° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE038761E1 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-43d7c9693da548749d9b5c0405c19c59 |
| Source note | uspto-grants-2005_07 |