HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → HCID 22349221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 22349231 | HCID 22349231 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 22349221 | HCID 22349221 | — |
Reaction Steps
A mixture of diethyl 5-(3-aminophenyl)-2-furanphosphonate (1 mmol), NBS (0.9 mmol) and AIBN (0.1 mmol) in 30 mL of CCl4 was stirred at rt for 2 h. Extraction and chromatography provided diethyl 5-(4-bromo-3-aminophenyl)-2-furanphosphonate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919322B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-998e93a9e89f4165a752a79460b8033a |
| Source note | uspto-grants-2005_07 |