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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 896002Generated: October 25, 2026

Bromotrimethylsilane → HCID 22349213, compound

https://huagongshe.com/reaction/896002

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBromotrimethylsilaneHCID 76113—
Reactant2,4-Dichloro-5-(diethylphosphonomethoxymethyl)thiazoleHCID 57457791—
ProductHCID 22349213HCID 22349213—

Reaction Steps

2,4-Dichloro-5-(diethylphosphonomethoxymethyl)thiazole was deesterified with TMSBr as described in Step D, Example 1, to provide the title compound (no. 14.01) as a solid. HPLC Rt=4.36 min; negative ion electrospray MS M−1 found: 276/278.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06919322B2
Source datasetuspto-grants-2005_07
ORD IDord-adff570e704d445cac0e890ae74d82eb
Source noteuspto-grants-2005_07