HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromotrimethylsilane → P-(2-Phenylethynyl)phosphonic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | HCID 11096651 | HCID 11096651 | — |
| Product | P-(2-Phenylethynyl)phosphonic acid | HCID 2063295 | — |
Reaction Steps
1-Diethylphosphono-2-phenylacetylene was deesterified with TMSBr as described in Step D, Example 1, to provide the title compound (no. 16.01) as a solid. HPLC Rt=3.75 min; negative ion electrospray MS M−1 found: 181.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919322B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-4cbc4d9d277a4dd58390be7a1f10839a |
| Source note | uspto-grants-2005_07 |