HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22349457, compound → HCID 22349479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22349457 | HCID 22349457 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22349479 | HCID 22349479 | 100.2% |
Reaction Steps
A mixture of 4-(4-methoxy-phenoxy)-2-methylnitrobenzene (3.5 grams, mmol) and methanol (200 mL) was treated with 200 miligrams of 10% palladium on carbon and was shaken under 50 psi of hydrogen gas for 3 hours. Filtration through a pad of celite and concentration in vacuo afforded 3.1 grams of 4-(4-methoxy-phenoxy)-2-methyl-phenylamine as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919332B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-dd3f1e8008e34fa0b6530b23a128de03 |
| Source note | uspto-grants-2005_07 |