HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 9906029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 68489806 | HCID 68489806 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 9906029 | HCID 9906029 | — |
Reaction Steps
The methyl (5R)-3-[4-(5,7-dihydro-6H-pyrrolo[3,4-b]pyridin-6-yl)-3-fluorophenyl]-2-oxo-5-oxazolidinecarboxylate (Step 1) is suspended in saturated ammonia in methanol (25 mL), stirred at ambient temperature for 4 h and filtered to give the title compound, mp 257° C. (dec.); MS (ESI+) for C17H15N4O3F m/z 343 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919329B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-5b7130418b844c5cb3a799d1a893c4d0 |
| Source note | uspto-grants-2005_07 |