(3-Aminopropyl)triethoxysilane → HCID 22345864, compound

HRID 896955Notes

Reaction equation

HRID 896955 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][Si:5]([O:12][CH2:13][CH3:14])([O:9][CH2:10][CH3:11])[O:6][CH2:7][CH3:8].[C:15]([O:19][C:20]([CH3:23])([CH3:22])[CH3:21])(=[O:18])[CH:16]=[CH2:17]>C(O)C>[C:20]([O:19][C:15]([CH2:16][CH2:17][NH:1][CH2:2][CH2:3][CH2:4][Si:5]([O:12][CH2:13][CH3:14])([O:6][CH2:7][CH3:8])[O:9][CH2:10][CH3:11])=[O:18])([CH3:23])([CH3:22])[CH3:21]

Participants

4

Reactant 2

HCID 13521(3-Aminopropyl)triethoxysilaneHCID 15458tert-Butyl acrylate

Product 1

HCID 22345864HCID 22345864, compoundYield 93%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In dehydrated ethanol, 22.1 g (100 mmol) of 3-aminopropyltriethoxysilane was dissolved, and to the solution, was added 12.8 g (100 mmol) of t-butyl acrylate, and the mixture was stirred at room temperature for 24 hours. After completion of the reaction, 32.5 g of the objective compound was obtained by removing solvent.

Workup

  1. customAfter completion of the reaction

Sources & evidence

ORD record
ord-9cde66726894479e93637b9118cb3a0f
Source dataset
uspto-grants-2005_07
Patent number
US06921623B2

Reaction notes

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